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The possibility to define a two-way relationship between age and a spectral property of ancient flax textiles has been investigated in the present paper employing both FT-IR and Raman analyses on selected samples dated from about 3250 B. In agreement with the kinetics theoretical model, the experimental relationships are of an exponential type, giving correlation coefficients higher than 0.9.

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For the first time, the possibility to define a correlation among spectral properties and age of flax samples, by using calibration curves, has been proved.

After a first selection to eliminate polluted samples, based on visual inspection, on proper mechanical tests and on a first glance at the resulting spectra, eleven samples of the original 14 have been used for Raman analysis and eight for FT-IR analysis.

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